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  • Dürig, WiebkeSwedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment (författare)

What is in the fish? Collaborative trial in suspect and non-target screening of organic micropollutants using LC- and GC-HRMS

  • Artikel/kapitelEngelska2023

Förlag, utgivningsår, omfång ...

  • Elsevier,2023
  • electronicrdacarrier

Nummerbeteckningar

  • LIBRIS-ID:oai:DiVA.org:umu-216197
  • https://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-216197URI
  • https://doi.org/10.1016/j.envint.2023.108288DOI
  • https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-225823URI
  • https://res.slu.se/id/publ/127606URI

Kompletterande språkuppgifter

  • Språk:engelska
  • Sammanfattning på:engelska

Ingår i deldatabas

Klassifikation

  • Ämneskategori:ref swepub-contenttype
  • Ämneskategori:art swepub-publicationtype

Anmärkningar

  • A collaborative trial involving 16 participants from nine European countries was conducted within the NORMAN network in efforts to harmonise suspect and non-target screening of environmental contaminants in whole fish samples of bream (Abramis brama). Participants were provided with freeze-dried, homogenised fish samples from a contaminated and a reference site, extracts (spiked and non-spiked) and reference sample preparation protocols for liquid chromatography (LC) and gas chromatography (GC) coupled to high resolution mass spectrometry (HRMS). Participants extracted fish samples using their in-house sample preparation method and/or the protocol provided. Participants correctly identified 9–69 % of spiked compounds using LC-HRMS and 20–60 % of spiked compounds using GC-HRMS. From the contaminated site, suspect screening with participants’ own suspect lists led to putative identification of on average ∼145 and ∼20 unique features per participant using LC-HRMS and GC-HRMS, respectively, while non-target screening identified on average ∼42 and ∼56 unique features per participant using LC-HRMS and GC-HRMS, respectively. Within the same sub-group of sample preparation method, only a few features were identified by at least two participants in suspect screening (16 features using LC-HRMS, 0 features using GC-HRMS) and non-target screening (0 features using LC-HRMS, 2 features using GC-HRMS). The compounds identified had log octanol/water partition coefficient (KOW) values from −9.9 to 16 and mass-to-charge ratios (m/z) of 68 to 761 (LC-HRMS and GC-HRMS). A significant linear trend was found between log KOW and m/z for the GC-HRMS data. Overall, these findings indicate that differences in screening results are mainly due to the data analysis workflows used by different participants. Further work is needed to harmonise the results obtained when applying suspect and non-target screening approaches to environmental biota samples.

Ämnesord och genrebeteckningar

Biuppslag (personer, institutioner, konferenser, titlar ...)

  • Lindblad, SofiaSwedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment (författare)
  • Golovko, OksanaSwedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment (författare)
  • Gkotsis, GeorgiosDepartment of Chemistry, National and Kapodistrian University of Athens, Athens, Greece (författare)
  • Aalizadeh, RezaDepartment of Chemistry, National and Kapodistrian University of Athens, Athens, Greece (författare)
  • Nika, Maria-ChristinaDepartment of Chemistry, National and Kapodistrian University of Athens, Athens, Greece (författare)
  • Thomaidis, NikolaosDepartment of Chemistry, National and Kapodistrian University of Athens, Athens, Greece (författare)
  • Alygizakis, Nikiforos A.Department of Chemistry, National and Kapodistrian University of Athens, Athens, Greece; Environmental Institute, Okružná 784/42, Koš, Slovakia (författare)
  • Plassmann, Merle,1981-Stockholms universitet,Institutionen för miljövetenskap(Swepub:su)mples (författare)
  • Haglund, PeterUmeå universitet,Kemiska institutionen(Swepub:umu)peha0004 (författare)
  • Fu, QiuguoEawag: Swiss Federal Institute of Aquatic Science and Technology, Überlandstrasse 133, Dübendorf, Switzerland; Helmholtz Centre for Environmental Research - UFZ, Permoserstraße 15, Leipzig, Germany (författare)
  • Hollender, JulianeEawag: Swiss Federal Institute of Aquatic Science and Technology, Überlandstrasse 133, Dübendorf, Switzerland; Institute of Biogeochemistry and Pollutant Dynamics, ETH Zürich, Universitätstrasse 16, Zürich, Switzerland (författare)
  • Chaker, JadeUniversité de Rennes, Inserm, EHESP, Irset - UMR_S, Rennes, France (författare)
  • David, ArthurUniversité de Rennes, Inserm, EHESP, Irset - UMR_S, Rennes, France (författare)
  • Kunkel, UweBavarian Environment Agency, Bürgermeister-Ulrich-Straße 160, Augsburg, Germany (författare)
  • Macherius, AndréBavarian Environment Agency, Bürgermeister-Ulrich-Straße 160, Augsburg, Germany (författare)
  • Belova, LidiaToxicological Centre, University of Antwerp, Universiteitsplein 1, Wilrijk, Belgium (författare)
  • Poma, GiuliaToxicological Centre, University of Antwerp, Universiteitsplein 1, Wilrijk, Belgium (författare)
  • Preud'Homme, HuguesIPREM-UMR5254, E2S UPPA, CNRS, 2 avenue Angot, Pau cedex, France (författare)
  • Munschy, CatherineIfremer, CCEM Contamination Chimique des Écosystèmes Marins, Nantes, France (författare)
  • Aminot, YannIfremer, CCEM Contamination Chimique des Écosystèmes Marins, Nantes, France (författare)
  • Jaeger, CarstenBundesanstalt für Materialforschung und -prüfung (BAM), Analytical Chemistry, Richard-Willstätter-Straße 11, Berlin, Germany (författare)
  • Lisec, JanBundesanstalt für Materialforschung und -prüfung (BAM), Analytical Chemistry, Richard-Willstätter-Straße 11, Berlin, Germany (författare)
  • Hansen, MartinDepartment of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark (författare)
  • Vorkamp, KatrinDepartment of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark (författare)
  • Zhu, LinyanDepartment of Environmental Science, Aarhus University, Frederiksborgvej 399, Roskilde, Denmark (författare)
  • Cappelli, FrancescaWater Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy (författare)
  • Roscioli, ClaudioWater Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy (författare)
  • Valsecchi, SaraWater Research Institute, National Research Council of Italy, Via del Mulino 19, MB, Brugherio, Italy (författare)
  • Bagnati, RenzoDepartment of Environmental Health Sciences, Istituto di Ricerche Farmacologiche Mario Negri IRCCS, Via Mario Negri 2, Milan, Italy (författare)
  • González, BelénDepartment of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain (författare)
  • Prieto, AiletteDepartment of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain (författare)
  • Zuloaga, OlatzDepartment of Analytical Chemistry, Faculty of Science and Technology, University of the Basque Country (UPV/EHU), Barrio Sarriena s/n, Leioa, Spain; Research Centre for Experimental Marine Biology and Biotechnology (PIE), University of the Basque Country (UPV/EHU), Areatza Pasealekua 47, Plentzia, Spain (författare)
  • Gil-Solsona, RubenCatalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Universitat de Girona, Girona, Spain; Institute of Environmental Assessment and Water Research – Severo Ochoa Excellence Center (IDAEA), Spanish Council of Scientific Research (CSIC), Barcelona 08034, Spain (författare)
  • Gago-Ferrero, PabloCatalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Institute of Environmental Assessment and Water Research – Severo Ochoa Excellence Center (IDAEA), Spanish Council of Scientific Research (CSIC), Barcelona 08034, Spain (författare)
  • Rodriguez-Mozaz, SaraCatalan Institute for Water Research (ICRA), Carrer Emili Grahit 101, Girona, Spain; Universitat de Girona, Girona, Spain (författare)
  • Budzinski, HélèneUniversity Bordeaux, CNRS, Bordeaux INP, EPOC, UMR 5805, Pessac, France (författare)
  • Devier, Marie-HeleneUniversity Bordeaux, CNRS, Bordeaux INP, EPOC, UMR 5805, Pessac, France (författare)
  • Dierkes, GeorgFederal Institute of Hydrology, Am Mainzer Tor 1, Koblenz, Germany (författare)
  • Boulard, LiseFederal Institute of Hydrology, Am Mainzer Tor 1, Koblenz, Germany; Metabolomics Core Facility, Centre de Ressources et Recherches Technologiques (C2RT), Institut Pasteur, 25-28 Rue du Dr Roux, Paris, France (författare)
  • Jacobs, GrietFlemish Institute for Technological Research (VITO), Unit Separation and Conversion Technology, Boeretang 200, Mol, Belgium (författare)
  • Voorspoels, StefanFlemish Institute for Technological Research (VITO), Unit Separation and Conversion Technology, Boeretang 200, Mol, Belgium (författare)
  • Rüdel, HeinzFraunhofer Institute for Molecular Biology and Applied Ecology (Fraunhofer IME), Auf dem Aberg 1, Schmallenberg, Germany (författare)
  • Ahrens, LutzSwedish University of Agricultural Sciences,Sveriges lantbruksuniversitet,Institutionen för vatten och miljö,Department of Aquatic Sciences and Assessment(Swepub:slu)50142 (författare)
  • Sveriges lantbruksuniversitetInstitutionen för vatten och miljö (creator_code:org_t)
  • Sveriges lantbruksuniversitet

Sammanhörande titlar

  • Ingår i:Environment International: Elsevier1810160-41201873-6750

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