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- Åberg, VeronicaUmeå universitet,Kemiska institutionen (author)
Synthesis and absolute configuration of methyl (-)-(3R)-8-(4-bromophenyl)-7-(naphthalen-1-ylmethyl)-5-oxo-2,3-dihydro-5H-thiazolo[3,2-a]pyridine-3-carboxylate
- Article/chapterEnglish2002
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- 2002
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- LIBRIS-ID:oai:DiVA.org:umu-9050
- https://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-9050URI
- https://doi.org/10.1107/S1600536802011480DOI
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- Language:English
- Summary in:English
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- The title molecule, C26H20BrNO3S, contains a ring-fused 2-pyridinone framework substituted with a 4-bromo-phenyl-, a naphthalen-1-ylmethyl and a methoxycarbonyl substituent. The main goal of this work was to confirm the stereochemistry for the methoxycarbonyl substituent, which proved to be 3R. Moreover, the 4-bromophenyl substituent was shown to be rotated out of the plane of the 2-pyridinone ring, with a torsion angle of 61.2 (5)°. To allow the best packing arrangement, the naphthalen-1-ylmethyl substituent is positioned to mediate an intermolecular - interaction.
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- NATURVETENSKAP Kemi hsv//swe
- NATURAL SCIENCES Chemical Sciences hsv//eng
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- Boström, Dan (author)
- Fischer, A (author)
- Almqvist, FredrikUmeå universitet,Kemiska institutionen(Swepub:umu)fral0001 (author)
- Umeå universitetKemiska institutionen (creator_code:org_t)
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- In:Acta Crystallographica Section E58:8, s. 812-8141600-5368
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