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Structural Assignment of σ-π-Palladium Complexes by 2D NMR
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- Gogoll, Adolf (author)
- Uppsala universitet,Organisk kemi
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- Grennberg, Helena (author)
- Uppsala universitet,Organisk kemi
- (creator_code:org_t)
- Wiley, 1993
- 1993
- English.
- In: Magnetic Resonance in Chemistry. - : Wiley. - 0749-1581 .- 1097-458X. ; 31:10, s. 954-959
- Journal article (peer-reviewed)
Abstract
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- A series of (σ-π)palladium complexes derived from cyclooctadiene were investigated by 1H, 13C and 19F NMR. The stereochemical assignment was based on intramolecular NOEs in conjunction with molecular modelling and semi-empirical methods, and confirmed by interligand NOEs in nitrogen chelate complexes derived from the title compounds. The nitrogen chelating ligands are involved in a rotation with respect to the ligand-palladium axis.
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