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  • Minelli, CaterinaNational Physical Laboratory (NPL) (author)

Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles

  • Article/chapterEnglish2022

Publisher, publication year, extent ...

  • 2022
  • Royal Society of Chemistry (RSC),2022
  • electronicrdacarrier

Numbers

  • LIBRIS-ID:oai:research.chalmers.se:433484d6-68bd-41c5-9658-5a80dc78d816
  • https://research.chalmers.se/publication/529202URI
  • https://doi.org/10.1039/d1nr07775aDOI
  • https://res.slu.se/id/publ/116589URI
  • http://kipublications.ki.se/Default.aspx?queryparsed=id:149061517URI

Supplementary language notes

  • Language:English
  • Summary in:English

Part of subdatabase

Classification

  • Subject category:art swepub-publicationtype
  • Subject category:ref swepub-contenttype

Notes

  • We describe the outcome of a large international interlaboratory study of the measurement of particle number concentration of colloidal nanoparticles, project 10 of the technical working area 34, "Nanoparticle Populations" of the Versailles Project on Advanced Materials and Standards (VAMAS). A total of 50 laboratories delivered results for the number concentration of 30 nm gold colloidal nanoparticles measured using particle tracking analysis (PTA), single particle inductively coupled plasma mass spectrometry (spICP-MS), ultraviolet-visible (UV-Vis) light spectroscopy, centrifugal liquid sedimentation (CLS) and small angle X-ray scattering (SAXS). The study provides quantitative data to evaluate the repeatability of these methods and their reproducibility in the measurement of number concentration of model nanoparticle systems following a common measurement protocol. We find that the population-averaging methods of SAXS, CLS and UV-Vis have high measurement repeatability and reproducibility, with between-labs variability of 2.6%, 11% and 1.4% respectively. However, results may be significantly biased for reasons including inaccurate material properties whose values are used to compute the number concentration. Particle-counting method results are less reproducibile than population-averaging methods, with measured between-labs variability of 68% and 46% for PTA and spICP-MS respectively. This study provides the stakeholder community with important comparative data to underpin measurement reproducibility and method validation for number concentration of nanoparticles.

Subject headings and genre

Added entries (persons, corporate bodies, meetings, titles ...)

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Related titles

  • In:Nanoscale: Royal Society of Chemistry (RSC)14, s. 4690-47042040-33722040-3364

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Minelli, Caterin ...
Wywijas, Magdale ...
Bartczak, Dorota
Cuello-Nunez, Su ...
Infante, Heidi G ...
Deumer, Jerome
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Gollwitzer, Chri ...
Krumrey, Michael
Murphy, Karen E.
Johnson, Monique ...
Bustos, Antonio ...
Strenge, Ingo H.
Faure, Bertrand
Hoghoj, Peter
Tong, Vivian
Burr, Loic
Norling, Karin, ...
Höök, Fredrik, 1 ...
Roesslein, Matth ...
Kocic, Jovana
Hendriks, Lyndse ...
Kestens, Vikram
Ramaye, Yannic
Lopez, Maria C. ...
Auclair, Guy
Mehn, Dora
Gilliland, Dougl ...
Potthoff, Annegr ...
Oelschlagel, Kat ...
Tentschert, Jutt ...
Jungnickel, Hara ...
Krause, Benjamin ...
Hachenberger, Yv ...
Reichardt, Phili ...
Luch, Andreas
Whittaker, Thoma ...
Stevens, Molly M ...
Gupta, Shalini
Singh, Akash
Lin, Fang-hsin
Liu, Yi-Hung
Costa, Anna Luis ...
Baldisserri, Car ...
Jawad, Rid
Andaloussi, Sami ...
Holme, Margaret ...
Lee, Tae Geol
Kwak, Minjeong
Kim, Jaeseok
Ziebel, Johanna
Guignard, Cedric
Cambier, Sebasti ...
Contal, Servane
Gutleb, Arno C.
Tatarkiewicz, Ja ...
Jankiewicz, Bart ...
Bartosewicz, Bar ...
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Fagan, Jeffrey A ...
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Runden-Pran, Eli ...
Dusinska, Maria
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Price, David
Nesbitt, Ian
O'Reilly, Sarah
Peters, Ruud J. ...
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Harrison, Angela ...
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Gering, Anne
McCarron, Eileen
Fitzgerald, Niam ...
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Tuoriniemi, Jani
Sakai, Midori
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Prina-Mello, Adr ...
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Adams, Jessica
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Panariello, Luca
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Valsami-Jones, E ...
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