WFRF:(Li Bing Hui)
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Intramolecularly two-centered cooperation catalysis for the synthesis of cyclic carbonates from CO2 and epoxides
- Zhang, Xiang (author)
- Jia, Yin-Bao (author)
- Lu, Xiao-Bing (author)
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- Li, Bo (author)
- Wang, Hui (author)
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- (creator_code:org_t)
- Elsevier BV, 2008
- 2008
- English.
- In: Tetrahedron Letters. - : Elsevier BV. - 0040-4039 .- 1359-8562. ; 49:46, s. 6589-6592
- Journal article (peer-reviewed)
Abstract
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- A catalyst systern containing an electrophilic center and a sterically hindered nUcleophilic center in one molecule was applied to the cycloaddition reaction of CO2 and epoxides. This intramolecularly two-centered cooperation catalyst showed activity even at a high [epoxide]/[catalyst] ratio up to 50000 under mild conditions such as solvent-free, ambient temperature, and low CO2 pressure. The reaction of CO2 with (S)-propylene oxide at 80 degrees C in the presence of the bifunctional catalyst gives (S)-propylene carbonate in 96% ee with retention of stereochemistry.
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- Zhang, Xiang
- Jia, Yin-Bao
- Lu, Xiao-Bing
- Li, Bo
- Wang, Hui
- Sun, Licheng
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- Tetrahedron Lett ...
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- Royal Institute of Technology
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