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Pulse-assisted homonuclear dipolar recoupling of half-integer quadrupolar spins in magic-angle spinning NMR
- Eden, M (author)
- Annersten, H (author)
-
- Zazzi, Åsa (author)
- KTH,Oorganisk kemi
- (creator_code:org_t)
- Elsevier BV, 2005
- 2005
- English.
- In: Chemical Physics Letters. - : Elsevier BV. - 0009-2614 .- 1873-4448. ; 410:1-3, s. 24-30
- Journal article (peer-reviewed)
Abstract
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- We demonstrate numerically and experimentally that zero-quantum homonuclear dipolar recoupling techniques employing rotor-synchronized 180 degrees pulses, previously introduced for spin-1/2 applications, are useful also for magnetization transfers between half-integer quadrupolar nuclei in rotating solids. The recoupling sequences are incorporated as mixing periods in two-dimensional experimental protocols, that correlate either single-quantum coherences of coupled spins, or triple-quantum with single-quantum coherences for improving spectral resolution. We present Na-23 and Al-27 NMR experiments on powders of sodium sulphite [Na2SO3], YAG [Y3Al5O12] and a synthetic chlorite mineral [Mg4.5Al3Si2.5O10(OH)(8)].
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- NATURVETENSKAP -- Kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences (hsv//eng)
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- Chemistry
- Kemi
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