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Fracture of Cr2O3 single crystals on the microscale

Harihara Subramonia Iyer, Anand, 1990 (author)
Chalmers tekniska högskola,Chalmers University of Technology
Stiller, Krystyna Marta, 1947 (author)
Chalmers tekniska högskola,Chalmers University of Technology
Hörnqvist Colliander, Magnus, 1979 (author)
Chalmers tekniska högskola,Chalmers University of Technology
 (creator_code:org_t)
Elsevier BV, 2021
2021
English.
In: Materialia. - : Elsevier BV. - 2589-1529. ; 15
  • Journal article (peer-reviewed)
Abstract Subject headings
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  • Studying cleavage properties of protective oxide scales is imperative to understand their fracture behaviour, since transgranular fracture is observed in many cases. The small thickness and polycrystalline structure of such scales makes it difficult to identify active cleavage planes directly from mechanical testing. To resolve this issue for Cr2O3, we present an approach to experimentally identify cleavage planes through micro-cantilever bending. Single crystal wafers are used to prepare micro-cantilevers of pentagonal cross-section in different orientations, targeting possible cleavage planes. Fracture surface imaging showed rhombohedral and pyramidal fracture, though surface energy studies predict rhombohedral as the dominant plane. There does exist a preference for rhombohedral fracture over pyramidal, which is also revealed from the experiments.

Subject headings

TEKNIK OCH TEKNOLOGIER  -- Maskinteknik -- Teknisk mekanik (hsv//swe)
ENGINEERING AND TECHNOLOGY  -- Mechanical Engineering -- Applied Mechanics (hsv//eng)
TEKNIK OCH TEKNOLOGIER  -- Materialteknik -- Keramteknik (hsv//swe)
ENGINEERING AND TECHNOLOGY  -- Materials Engineering -- Ceramics (hsv//eng)
TEKNIK OCH TEKNOLOGIER  -- Materialteknik -- Annan materialteknik (hsv//swe)
ENGINEERING AND TECHNOLOGY  -- Materials Engineering -- Other Materials Engineering (hsv//eng)

Keyword

Micromechanics
fracture behavior
chromia
Ceramics
electron microscopy
single crystal

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ref (subject category)

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