Sökning: onr:"swepub:oai:research.chalmers.se:f2cf64a4-cbe5-4ec0-950b-f3dc3c1c6514" > Solvent-free synthe...
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000 | 04221naa a2200529 4500 | |
001 | oai:research.chalmers.se:f2cf64a4-cbe5-4ec0-950b-f3dc3c1c6514 | |
003 | SwePub | |
008 | 220614s2022 | |||||||||||000 ||eng| | |
024 | 7 | a https://doi.org/10.1016/j.molliq.2022.1193582 DOI |
024 | 7 | a https://research.chalmers.se/publication/5307852 URI |
040 | a (SwePub)cth | |
041 | a engb eng | |
042 | 9 SwePub | |
072 | 7 | a art2 swepub-publicationtype |
072 | 7 | a ref2 swepub-contenttype |
100 | 1 | a Maurina Morais, Eduardo,d 1989u Chalmers tekniska högskola,Chalmers University of Technology4 aut0 (Swepub:cth)maurina |
245 | 1 0 | a Solvent-free synthesis of protic ionic liquids. Synthesis, characterization and computational studies of triazolium based ionic liquids |
264 | 1 | b Elsevier BV,c 2022 |
338 | a electronic2 rdacarrier | |
520 | a A series of triazolium and imidazolium based protic ionic liquids were synthesized using a solvent-free method designed to address several limitations encountered with other commonly used methods. Using this method, pure (98–99% m/m) and dry (128–553 ppm of water) protic ionic liquids were synthesized (in a laboratory scale) without the need for purification methods that require heating the ionic liquid, hence avoiding the common issue of thermal decomposition. This method was also designed to allow for the accurate measurement of acid and base, and for the controlled mixing of both compounds, which is essential to avoid producing impure protic ionic liquids with excess of either acid or base. The system is constructed of only glass and chemically resistant polymer (PTFE and PVDF) parts, which avoid other contaminants that can result from unwanted reactions involving the reagents with common laboratory tools (metallic objects, paper, plastic, etc.). This process is described in detail in the paper as well as in a video. The resulting ionic liquids were carefully analyzed by spectroscopic and thermal methods designed to avoid water absorption, which is known to affect their properties. To complement this experimental characterization, computational chemistry tools were used to assess the ionic liquids’ properties, as well as to assign vibrational modes. | |
650 | 7 | a NATURVETENSKAPx Kemix Oorganisk kemi0 (SwePub)104042 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Inorganic Chemistry0 (SwePub)104042 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Fysikalisk kemi0 (SwePub)104022 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Physical Chemistry0 (SwePub)104022 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Materialkemi0 (SwePub)104032 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Materials Chemistry0 (SwePub)104032 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Annan kemi0 (SwePub)104992 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Other Chemistry Topics0 (SwePub)104992 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Teoretisk kemi0 (SwePub)104072 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Theoretical Chemistry0 (SwePub)104072 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemi0 (SwePub)1042 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciences0 (SwePub)1042 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Organisk kemi0 (SwePub)104052 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Organic Chemistry0 (SwePub)104052 hsv//eng |
653 | a Synthesis | |
653 | a Protic Ionic Liquid | |
653 | a DFT | |
653 | a Acidity | |
653 | a Solvent-free | |
653 | a Vibrational Assignment | |
700 | 1 | a Abdurrokhman, Iqbaal,d 1991u Chalmers tekniska högskola,Chalmers University of Technology4 aut0 (Swepub:cth)iqbaal |
700 | 1 | a Martinelli, Anna,d 1978u Chalmers tekniska högskola,Chalmers University of Technology4 aut0 (Swepub:cth)annamart |
710 | 2 | a Chalmers tekniska högskola4 org |
773 | 0 | t Journal of Molecular Liquidsd : Elsevier BVg 360q 360x 0167-7322 |
856 | 4 | u https://research.chalmers.se/publication/530802/file/530802_Fulltext.pdfx primaryx freey FULLTEXT |
856 | 4 8 | u https://doi.org/10.1016/j.molliq.2022.119358 |
856 | 4 8 | u https://research.chalmers.se/publication/530785 |
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