Search: L773:1615 4150 OR L773:1615 4169 > Total Synthesis of ...
Fältnamn | Indikatorer | Metadata |
---|---|---|
000 | 03929naa a2200529 4500 | |
001 | oai:DiVA.org:kth-148291 | |
003 | SwePub | |
008 | 140805s2014 | |||||||||||000 ||eng| | |
009 | oai:DiVA.org:miun-22585 | |
009 | oai:DiVA.org:su-106068 | |
024 | 7 | a https://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-1482912 URI |
024 | 7 | a https://doi.org/10.1002/adsc.2013011482 DOI |
024 | 7 | a https://urn.kb.se/resolve?urn=urn:nbn:se:miun:diva-225852 URI |
024 | 7 | a https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-1060682 URI |
040 | a (SwePub)kthd (SwePub)miund (SwePub)su | |
041 | a engb eng | |
042 | 9 SwePub | |
072 | 7 | a ref2 swepub-contenttype |
072 | 7 | a art2 swepub-publicationtype |
100 | 1 | a Anderson, Mattiasu KTH,Industriell bioteknologi,AlbaNova Univ Ctr, KTH Royal Inst Technol, Sch Biotechnol, Div Ind Biotechnol, SE-10691 Stockholm, Sweden4 aut0 (Swepub:kth)u1eqa8pn |
245 | 1 0 | a Total Synthesis of Capsaicin Analogues from Lignin-Derived Compounds by Combined Heterogeneous Metal, Organocatalytic and Enzymatic Cascades in One Pot |
264 | c 2014-04-15 | |
264 | 1 | b Wiley,c 2014 |
338 | a print2 rdacarrier | |
500 | a QC 20140807 | |
500 | a AuthorCount:4; | |
520 | a The total synthesis of capsaicin analogues was performed in one pot, starting from compounds that can be derived from lignin. Heterogeneous palladium nanoparticles were used to oxidise alcohols to aldehydes, which were further converted to amines by an enzyme cascade system, including an amine transaminase. It was shown that the palladium catalyst and the enzyme cascade system could be successfully combined in the same pot for conversion of alcohols to amines without any purification of intermediates. The intermediate vanillyl-amine, prepared with the enzyme cascade system, could be further converted to capsaicin analogues without any purification using either fatty acids and a lipase, or Schotten-Baumann conditions, in the same pot. An aldol compound (a simple lignin model) could also be used as starting material for the synthesis of capsaicin analogues. Using l-alanine as organocatalyst, vanillin could be obtained by a retro-aldol reaction. This could be combined with the enzyme cascade system to convert the aldol compound to vanillylamine in a one-step one-pot reaction. | |
650 | 7 | a TEKNIK OCH TEKNOLOGIERx Industriell bioteknikx Bioprocessteknik0 (SwePub)209012 hsv//swe |
650 | 7 | a ENGINEERING AND TECHNOLOGYx Industrial Biotechnologyx Bioprocess Technology0 (SwePub)209012 hsv//eng |
650 | 7 | a NATURVETENSKAPx Kemix Organisk kemi0 (SwePub)104052 hsv//swe |
650 | 7 | a NATURAL SCIENCESx Chemical Sciencesx Organic Chemistry0 (SwePub)104052 hsv//eng |
653 | a aldol reaction | |
653 | a amine transferase | |
653 | a biocatalysis | |
653 | a capsaicin analogues | |
653 | a oxidation | |
653 | a palladium | |
653 | a renewable resources | |
700 | 1 | a Afewerki, Samsonu Mittuniversitetet,Avdelningen för naturvetenskap4 aut0 (Swepub:miun)samafe |
700 | 1 | a Berglund, Peru KTH,Industriell bioteknologi,AlbaNova Univ Ctr, KTH Royal Inst Technol, Sch Biotechnol, Div Ind Biotechnol, SE-10691 Stockholm, Sweden4 aut0 (Swepub:kth)u1271chh |
700 | 1 | a Cordova, Armandou Stockholms universitet,Mittuniversitetet,Avdelningen för naturvetenskap,Stockholm Univ, Dept Organ Chem, Arrhenius Lab, SE-10691 Stockholm, Sweden,Institutionen för organisk kemi,Mid Sweden University, Sweden4 aut0 (Swepub:su)acr |
710 | 2 | a KTHb Industriell bioteknologi4 org |
773 | 0 | t Advanced Synthesis and Catalysisd : Wileyg 356:9, s. 2113-2118q 356:9<2113-2118x 1615-4150x 1615-4169 |
856 | 4 8 | u https://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-148291 |
856 | 4 8 | u https://doi.org/10.1002/adsc.201301148 |
856 | 4 8 | u https://urn.kb.se/resolve?urn=urn:nbn:se:miun:diva-22585 |
856 | 4 8 | u https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-106068 |
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