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Salicylamide and salicylglycine oxidovanadium complexes with insulin-mimetic properties.
- Nilsson, Jessica (author)
- Shteinman, Albert A (author)
-
- Degerman, Eva (author)
- Lund University,Lunds universitet,Signaltransduktionsforskning,Forskargrupper vid Lunds universitet,Insulin Signal Transduction,Lund University Research Groups
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- Enyedy, Eva A (author)
- Kiss, Tamás (author)
- Behrens, Ulrich (author)
- Rehder, Dieter (author)
- Nordlander, Ebbe (author)
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- (creator_code:org_t)
- Elsevier BV, 2011
- 2011
- English.
- In: Journal of Inorganic Biochemistry. - : Elsevier BV. - 1873-3344 .- 0162-0134. ; 105, s. 1795-1800
- Journal article (peer-reviewed)
Abstract
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- Reaction of N-(2-hydroxybenzyl)-N-(2-picolyl) glycine (H(2)papy) with VOSO(4) in water gives the oxidovanadium(V) oxido-bridged dimer [{(papy)(VO)}(2) μ-O)] (1). Similarly, reaction of N-(2-hydroxybenzyl) glycine (H(2)glysal) with VOSO(4) gives [(glysal)VO(H(2)O)] (2) and reaction of salicylamide (Hsalam) with VOSO(4) in methanol gives [(salam)(2)VO] (3). The crystal structure of the oxido-bridged complex 1 is reported. The insulin-mimetic activity of all three complexes was evaluated with respect to their ability to phosphorylate protein kinase B (PKB). The speciations of complexes 1 and 2 were studied over the pH range 2-10. Complex 1 shows greater stability over the whole pH range but only 2 and 3 exhibit an insulin-mimetic effect.
Subject headings
- NATURVETENSKAP -- Biologi -- Biokemi och molekylärbiologi (hsv//swe)
- NATURAL SCIENCES -- Biological Sciences -- Biochemistry and Molecular Biology (hsv//eng)
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- ref (subject category)
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- Kiss, Tamás
- Behrens, Ulrich
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- Rehder, Dieter
- Nordlander, Ebbe
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