WFRF:(Wennerberg Johan)
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A practical and environmentally friendly protocol for synthesis of α-deuterated carboxylic acids
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- Wennerberg, Johan (author)
- Lund University,Lunds universitet,Centrum för analys och syntes,Kemiska institutionen,Institutioner vid LTH,Lunds Tekniska Högskola,Centre for Analysis and Synthesis,Department of Chemistry,Departments at LTH,Faculty of Engineering, LTH,Red Glead Discovery AB
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- Dreisch, Klaus (author)
- Red Glead Discovery AB
- (creator_code:org_t)
- 2023-03-02
- 2023
- English 7 s.
- In: Journal of Labelled Compounds and Radiopharmaceuticals. - : Wiley. - 0362-4803 .- 1099-1344. ; 66:4-6, s. 138-144
- Journal article (peer-reviewed)
Abstract
Subject headings
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- α-deuterated carboxylic acids have been synthesized from the corresponding malonic acids via hydrogen/deuterium exchange and decarboxylation in presence of D2O. The method is general, mild and efficient and does not require organic solvents or other additives. Yields range between 83% and 94% and purification was not necessary. Starting materials were easy accessible and the α-deuterated carboxylic acids may easily be transformed to other labeled compounds such as alcohols, aldehydes, esters, and amides. Characterization with NMR confirmed purity and isotopic purity.
Subject headings
- NATURVETENSKAP -- Kemi -- Organisk kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Organic Chemistry (hsv//eng)
Keyword
- H labeling
- decarboxylation
- malonic acids
- α-deuterated carboxylic acid
Publication and Content Type
- art (subject category)
- ref (subject category)
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