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LIBRIS Formathandbok  (Information om MARC21)
FältnamnIndikatorerMetadata
00002476naa a2200409 4500
001oai:DiVA.org:kth-29463
003SwePub
008110202s2010 | |||||||||||000 ||eng|
024a https://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-294632 URI
024a https://doi.org/10.1016/j.jallcom.2010.04.1432 DOI
040 a (SwePub)kth
041 a engb eng
042 9 SwePub
072 7a ref2 swepub-contenttype
072 7a art2 swepub-publicationtype
100a Baykal, A.4 aut
2451 0a Polyol synthesis of (polyvinylpyrrolidone) PVP-Mn3O4 nanocomposite
264 1b Elsevier BV,c 2010
338 a print2 rdacarrier
500 a QC 20110208
520 a We report on the synthesis of (polyvinylpyrrolidone) PVP-Mn3O4 nanocomposite via a polyol route. Crystalline phase was identified as Mn3O4 and the crystallite size was obtained as 6 +/- 1 nm from X-ray line profile fitting. Average particle size of 6.1 +/- 0.1 nm obtained from TEM analysis reveals nearly single crystalline nature of these nanoparticles in the composite. The capping of PVP around Mn3O4 nanoparticles was confirmed by FT-IR spectroscopy, the interaction being via bridging oxygens of the carbonyl (C=O) and the nanoparticle surface. T-C and T-B for PVP-Mn3O4 nanocomposite were observed at 42K and 28.5 K, respectively. The sample has hysteresis with small coercivity and remanent magnetization at 40K, resembling the superparamagnetic state. ac conductivity measurements on PVP-Mn3O4 nanocomposite revealed a conductivity in the order of 10(-7) S cm(-1) at lower frequencies. The conductivity change with respect to frequency can be explained by electronic exchange occurring between Mr(+2) and Mn+3 existing in sublattice of spinel lattice.
653 a Nanocomposite
653 a Nanomagnetic materials
653 a ac conductivity
653 a Magnetization
653 a TECHNOLOGY
653 a TEKNIKVETENSKAP
700a Bitrak, N.4 aut
700a Ünal, B.4 aut
700a Kavas, H.4 aut
700a Durmus, Z.4 aut
700a Özden, S.4 aut
700a Toprak, Muhammet S.u KTH,Funktionella material, FNM4 aut0 (Swepub:kth)u1u3m5a2
710a KTHb Funktionella material, FNM4 org
773t Journal of Alloys and Compoundsd : Elsevier BVg 502:1, s. 199-205q 502:1<199-205x 0925-8388x 1873-4669
8564 8u https://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-29463
8564 8u https://doi.org/10.1016/j.jallcom.2010.04.143

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