WFRF:(O' Brien T)
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Synthesis, Characterization, and Thermal Study of Divalent Germanium, Tin, and Lead Triazenides as Potential Vapor Deposition Precursors
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- Samii, Rouzbeh (author)
- Linköpings universitet,Kemi,Tekniska fakulteten
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- Zanders, David (author)
- Carleton Univ, Canada; Ruhr Univ Bochum, Germany
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- Fransson, Anton (author)
- Linköpings universitet,Halvledarmaterial,Tekniska fakulteten
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- (creator_code:org_t)
- 2021-08-06
- 2021
- English.
- In: Inorganic Chemistry. - : American Chemical Society (ACS). - 0020-1669 .- 1520-510X. ; 60:17, s. 12759-12765
- Journal article (peer-reviewed)
Abstract
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- Only a few M-N bonded divalent group 14 precursors are available for vapor deposition, in particular for Ge and Pb. A majority of the reported precursors are dicoordinated with the Sn(II) amidinates, the only tetracoordinated examples. No Ge(II) and Pb(II) amidinates suitable for vapor deposition have been demonstrated. Herein, we present tetracoordinated Ge(II), Sn(II), and Pb(II) complexes bearing two sets of chelating 1,3-di-tert-butyltriazenide ligands. These compounds are thermally stable, sublime quantitatively between 60 and 75 degrees C (at 0.5 mbar), and show ideal single-step volatilization by thermogravimetric analysis.
Subject headings
- NATURVETENSKAP -- Kemi -- Oorganisk kemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Inorganic Chemistry (hsv//eng)
- NATURVETENSKAP -- Kemi -- Materialkemi (hsv//swe)
- NATURAL SCIENCES -- Chemical Sciences -- Materials Chemistry (hsv//eng)
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- ref (subject category)
- art (subject category)
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- Samii, Rouzbeh
- Zanders, David
- Fransson, Anton
- Bacic, Goran
- Barry, Sean T.
- Ojamäe, Lars
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- Kessler, Vadim
- Pedersen, Henrik
- O´Brien, Nathan
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- Linköping University
- Swedish University of Agricultural Sciences
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